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Consequently, when the pH of the buffer is 7, the emission of 89 possesses the CIE coordinates of (0.41, 0.40) after excitation at 300 nm (Figure 28a, inset).


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The combined organic layers were stirred for 25 minutes with saturated NaHCO3 (sat. 40 L soln., pH 6-7). The organic and aqueous layers were separated, with the aqueous layer extracted again with TBME (20 L). The combined organic layers were extracted with saturated NaHC03 (40 L, pH 9). Analysis by'H NMR showed no residual acetic anhydride.